合成路线
![(4R,5S,6R)-6-[(t-butyldimethylsilyl)oxy]-5-[3-{(t-butyldimethylsilyl)oxy}propoxy]oct-7-en-1-yn-4-ol](https://cdn-oss.0elem.com/prod/mob/images/299/299411-13-5.jpg)
(4R,5S,6R)-6-[(t-butyldimethylsilyl)oxy]-5-[3-{(t-butyldimethylsilyl)oxy}propoxy]oct-7-en-1-yn-4-ol
CAS号：299411-13-5
英文名：(4R,5S,6R)-6-[(t-butyldimethylsilyl)oxy]-5-[3-{(t-butyldimethylsilyl)oxy}propoxy]oct-7-en-1-yn-4-ol
分子式：C23H46O4Si2
分子量：442.78
![methyl 6-bromo-2,4-bis-(O-tert-butyldimethylsilyl)-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside](https://cdn-oss.0elem.com/prod/mob/images/299/299411-01-1.jpg)
![methyl 6-bromo-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside](https://cdn-oss.0elem.com/prod/mob/images/299/299410-99-4.jpg)
![(2R,3S,4R)-4-[(t-butyldimethylsilyl)oxy]-3-[3-{(t-butyldimethylsilyl)oxy}propoxy]hex-5-ene-1,2-diol](https://cdn-oss.0elem.com/prod/mob/images/299/299411-05-5.jpg)
![(R)-2-{(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-but-3-enyl}-oxirane](https://cdn-oss.0elem.com/prod/mob/images/299/299411-09-9.jpg)
![methyl 6-bromo-4-(O-tert-butyldimethylsilyl)-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside](https://cdn-oss.0elem.com/prod/mob/images/299/299411-03-3.jpg)
上游原料
(2R,3S,4R)-4-[(t-butyldimethylsilyl)oxy]-3-[3-{(t-butyldimethylsilyl)oxy}propoxy]hex-5-ene-1,2-diol
methyl 6-bromo-4-(O-tert-butyldimethylsilyl)-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside
methyl 6-bromo-2,4-bis-(O-tert-butyldimethylsilyl)-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside
methyl 4,6-O-benzylidene-2,3-anhydro-β-mannopyranoside
methyl 6-bromo-3-O-[3-{(tert-butyldimethylsilyl)oxy}propyl]-6-deoxy-α-D-altropyranoside
(R)-2-{(1S,2R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-[3-(tert-butyl-dimethyl-silanyloxy)-propoxy]-but-3-enyl}-oxirane
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